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Parlar, H.A. ; Hustert, K. ; Gaeb, S. ; Korte, F.

Isolation, identification, and chromatographic characterization of some chlorinated C10 hydrocarbons in technical chlordane.

J. Agric. Food Chem. 27, 278-283 (1979)
DOI
Open Access Green möglich sobald Postprint bei der ZB eingereicht worden ist.
With the help of column chromatography, 3 new substances, 1-exo,4,5,7,8,8- hexachloro-3a,4,7,7a-tetrahydro-4,7-methanoindene 1-exo,2-exo,4,5,7,8,8- heptachloro-3a,4,7,7a-tetrahydro-4,7-methanoindane, and 1-exo,2-exo,4,6,7,8,8-heptachloro-3a,4,7,7a-tetrahydro-4,7-methanoindane, were isolated from technical chlordane and were identified by spectroscopic methods (mass spectrometry, infrared, and 1H NMR). These compounds could be synthesized by photochemical dechlorination of heptachlor and of α- (or cis-) chlordane in methanol. In addition, the mixture was investigated by capillary gas chromatography and by combined gas chromatography and mass spectrometry. The data obtained were used to characterize the composition of technical chlordane.
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Publikationstyp Artikel: Journalartikel
Dokumenttyp Wissenschaftlicher Artikel
ISSN (print) / ISBN 0021-8561
e-ISSN 1520-5118
Zeitschrift Journal of Agricultural and Food Chemistry
Quellenangaben Band: 27, Heft: 2, Seiten: 278-283 Artikelnummer: , Supplement: ,
Verlag American Chemical Society (ACS)
Begutachtungsstatus Peer reviewed
Institut(e) Institute of Ecological Chemistry (IOEC)