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Open Access Green möglich sobald Postprint bei der ZB eingereicht worden ist.
Structural elucidation of an octachloro component of technical chlordane (compound K) by spectroscopic and X-ray methods.
J. Agric. Food Chem. 25, 1365-1371 (1977)
The technical chlordane constituent designated compound K is a formal isomer of chlordane (C10H6Cl8) which is formed by chlorination of α-chlordene (1) (C10H6Cl6) via a Wagner-Meerwein rearrangement. Structural elucidation of K involves dechlorination reactions, especially spectroscopic studies (MS, 1H NMR, and 13C NMR) of various photodechlorination products (3-7). From these data a structure for compound K is proposed. Confirmation of this structure is obtained by single-crystal x-ray diffraction. According to the results, compound K corresponds to 2,4,4,5,6,6,7,8-octachlorooctahydro-1,5-ethenopentalene (2).
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Publikationstyp
Artikel: Journalartikel
Dokumenttyp
Wissenschaftlicher Artikel
ISSN (print) / ISBN
0021-8561
e-ISSN
1520-5118
Zeitschrift
Journal of Agricultural and Food Chemistry
Quellenangaben
Band: 25,
Heft: 6,
Seiten: 1365-1371
Verlag
American Chemical Society (ACS)
Nichtpatentliteratur
Publikationen
Begutachtungsstatus
Peer reviewed