PuSH - Publication Server of Helmholtz Zentrum München: Analysis of cyanogenic glycosides by micellar capillary electrophoresis.

Information

Clues to quality of journals

Open Access Policy of Helmholtz Association 2016

CC Licencences

Publication Metrics

Navigation

Home

Deutsch

EVA: Electronic Publishing

New EVA Application

Research

Advanced Search

Browse by ...

... HMGU-Authors/Consortia

... Organizational Structure

... Journal

... Publication Type

... Research Data

... Arbeitsgruppen

... Publication Year

Publication overview

Statistics

Statistics (last 5 years)

OA Publications

Publish

Submit Publication

Import publication from...

...EVA

Report missing publication

Highlights

Support & Contact

Contact persons

Help

Data protection

Helmholtz Open Science

JANE Journal Estimator

SHERPA/RoMEO

DOAJ

Export:

Text

Endnote (RIS) BIB

BibTeX

Campa, C.* ; Schmitt-Kopplin, P. ; Cataldi, T.R.I.* ; Bufo, S.A.* ; Freitag, D. ; Kettrup, A.

Analysis of cyanogenic glycosides by micellar capillary electrophoresis.

J. Chromatogr. A 739, 95-100 (2000)

Open Access Green as soon as Postprint is submitted to ZB.

Abstract
Metrics
Extra information

he separation of amygdalin, prunasin and their isomers neoamygdalin and sambunigrin could be achieved with micellar capillary electrophoresis (MEKC). The two isomers were obtained in alkaline conditions and were produced in less than 15 min at pH 11.0. The developed methods showed a good selectivity in the separation of the isomers only in the presence of SDS micelles. The working pH was optimized to allow best resolution and quantitative analysis of these compounds, With a linear calibration over an injection time from 1 to 20 s, the detection limit was found to be in the range of 5 mu M (S/N=3; 20 a injection time). Two pH buffer systems (pH 5.2 and pH 9.1) were chosen to confirm the peak attributions of the compounds in the apple and peach seeds samples. Sambunigrin was found in both apple and peach seeds but could not be quantified because of missing standards. Prunasin and amygdalin were not found in the apple sample, while they were quantified in the peach seeds in concentrations of 50 mu g/g and 90 mu g/g (dry weight), respectively.

Impact Factor

Scopus SNIP

2.520

0.000