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Sandrock, K. ; Attar, A. ; Bieniek, D.

Synthese 14C-markierter Umweltchemikalen.

Synthesis of 14 C labeled environment contaminants.

J. Labelled Comp. Radiopharm. 14, 197-204 (1978)
DOI
Open Access Green as soon as Postprint is submitted to ZB.
Upon the reaction of benzene-14C via nitrobenzene-14C and aniline-14C, some 14C-labelled environmental contaminants were were synthesized. By chlorination of aniline-14C and acetanilide-14C the authors prepared chloroanilines-14C. Gomberg-Bachmann or Cadogan reaction of diazotated chloroanilines-14C with different chlorobenzenes gave di, tri- and pentachlorobiphenyls-14C. By boiling anilinediazonium sulfate-14C the authors prepared phenol-14C, which was chlorinated to give 2,4,6-trichlorophenol-14C. Hexachlorobenzene-14C and pentachloronitrobenzene-14C were prepared by chlorination of nitrobenzene- 14C. Chloralkylene 9-14C was synthesized by Friedel-Crafts alkylation of 2,4'-dichlorobiphenyl-14C with 2-chloropropane.
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Publication type Other: Correction, Addition
Corresponding Author
Keywords Pentachloronitrobenzene; Hexachlorobenzene; Pentachloro
ISSN (print) / ISBN 0362-4803
e-ISSN 1099-1344
Journal Journal of Labelled Compounds and Radiopharmaceuticals
Quellenangaben Volume: 14, Issue: 2, Pages: 197-204 Article Number: , Supplement: ,
Publisher Wiley
Non-patent literature Publications
Reviewing status Peer reviewed
Institute(s) Institute of Ecological Chemistry (IOEC)