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Open Access Green as soon as Postprint is submitted to ZB.
Isolation, identification, and chromatographic characterization of some chlorinated C10 hydrocarbons in technical chlordane.
J. Agric. Food Chem. 27, 278-283 (1979)
With the help of column chromatography, 3 new substances, 1-exo,4,5,7,8,8- hexachloro-3a,4,7,7a-tetrahydro-4,7-methanoindene 1-exo,2-exo,4,5,7,8,8- heptachloro-3a,4,7,7a-tetrahydro-4,7-methanoindane, and 1-exo,2-exo,4,6,7,8,8-heptachloro-3a,4,7,7a-tetrahydro-4,7-methanoindane, were isolated from technical chlordane and were identified by spectroscopic methods (mass spectrometry, infrared, and 1H NMR). These compounds could be synthesized by photochemical dechlorination of heptachlor and of α- (or cis-) chlordane in methanol. In addition, the mixture was investigated by capillary gas chromatography and by combined gas chromatography and mass spectrometry. The data obtained were used to characterize the composition of technical chlordane.
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Publication type
Article: Journal article
Document type
Scientific Article
Language
english
Publication Year
1979
HGF-reported in Year
0
ISSN (print) / ISBN
0021-8561
e-ISSN
1520-5118
Quellenangaben
Volume: 27,
Issue: 2,
Pages: 278-283
Publisher
American Chemical Society (ACS)
Reviewing status
Peer reviewed
Institute(s)
Institute of Ecological Chemistry (IOEC)
Scopus ID
0018426562
Erfassungsdatum
1979-12-31