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Xu, Y. ; Lorenz, W.G. ; Pfister, G. ; Bahadir, M.A. ; Korte, F.

Residue analysis of triazine herbicides in soil: Comparison of a capillary gas chromatographic and a high-performance liquid chromatographic method.

Fresenius Z. Anal. Chem. 325, 377-380 (1986)

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Two methods for the determination of triazines in soil were developed and compared. After extraction of the residues with methanol and clean-up by gel permeation chromatography, the samples evaporated were analysed for triazines by splitless capillary gas-chromatography with NP-detector (GC-NPD) and microbore high performance liquid chromatography with UV detector (HPLC-UV) at 222 nm. Both methods gave similar results. The microbore HPLC method was suitable for the analysis of a number of triazines at 10 ppb whereas capillary GC method was used for the analysis of triazines at 5 ppb. Satisfactory average recoveries for the two methods were obtained at 80 ppb and 20 ppb, respectively.

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